Densities and Viscosities of Oleic Acid at Atmospheric Pressure

The densities of oleic acid were measured over the temperature range from (293 to 459) K at atmospheric pressure using a densimeter based on the modified hydrostatic weighing method. The dynamic viscosities of the same oleic acid sample were measured using a capillary viscometer (VPZ-2 m) in the range from (293 to 363) K at atmospheric pressure. The combined expanded uncertainty of the density, atmospheric pressure, viscosity, and temperature measurements at the 95% confidence level with a coverage factor of k = 2 is estimated to be 0.15%, 1.0%, 3.5%, and 15 mK, respectively. The values of uncertainty for density and viscosity include the effects of purity and calibration (total expanded uncertainty). These experimental data were used to develop wide-range correlations for the density and viscosity based on theoretically confirmed Arrhenius–Andrade and Vogel-Tamman-Fulcher (VTF) models. The value of the glass temperature ( T _g= 179.78 K.) for the oleic acid was estimated using the VTF parameters derived from the present viscosity measurements. To additionally validate the reliability of the measured density data, the same oleic acid samples were measured using the pycnometric method. The present study showed that the densities measured using the modified hydrostatic weighing densimeter (HWD) agree with the values obtained using the pycnometric method within 0.09% for Sample 1 and 0.25% for Sample 2.     

Preparation of CaO granules using the granulation method

ABSTRACT

Improving the hydration resistance of CaO particle in manufacturing and application of free CaO-containing materials has practical significance. In this study, CaO granules was made from Ca(OH)₂ particles, which were fabricated by the granulation method. The results showed that the hydration resistance of the CaO granules which was prepared under 1700?r?min^?1 was the best, the CaO granules was sintered well in calcination process, the shell of CaO granules was relatively dense, which improves the hydration resistance of CaO granules, and the rate of hydration weight increment was 0.58% after placed in the air for 20 days under a temperature of 10–14°C and a relative humidity of 57–81%.     

RI/VI联用测定聚乙烯相对分子质量及其分布

150℃测试温度下，以1，2，4-三氯苯为溶剂，采用示差折光指数器，毛细管黏度计双检测器联用凝胶渗透色谱技术测定了聚乙烯的相对分子质量及其分布。与常规凝胶渗透色谱法对比，该方法不仅能直接得到聚乙烯较精确的相对分子质量和分布形态，同时可以得到聚乙烯的特性黏数分布。     

Simultaneous Measurement of Viscosity and Density with an Oscillating-Disk Instrument: The Effect of Fixed Plates

The period and damping of the free motion of a body oscillating in a fluid depend on the fluid's viscosity and density. Commonly, a working equation which expresses the damping as a function of the viscosity and density is solved for the viscosity, the damping being measured and the density being treated as an independently supplied parameter. Another working equation exists for the period, and, in general, the period depends on a combination of the viscosity and the density which is linearly independent of the combination that appears in the damping equation. It is, therefore, in principle, possible to determine both the viscosity and the density by a simultaneous solution of the two coupled working equations, since the period also is measured. In this paper, the working equations that describe the oscillating-disk viscometer are reviewed and their simultaneous solution is considered. The effect of fixed plates symmetrically located above and below the oscillating disk is of specific interest. The paper's main result is that fixed plates can dramatically increase the independence of the damping and period working equations, so that it becomes indeed feasible to determine the viscosity and the density of a fluid simultaneously from the damping and period of oscillating motion. A price is paid, however, because the instrument's working equations when plates are present have multiple solutions. Under special conditions, these multiple solutions can coalesce, and then one can only deduce the viscosity from the damping equation if the density is known a priori.     

石油沥青60℃动力粘度测定影响因素的探讨

粘度是表征沥青稠度的一个重要指标。通过论述石油沥青粘度测定法(真空毛细管法)中毛细管的选择、温度、真空度、取样量等对试验结果的影响及试验过程中的其它注意事项,表明了在测定石油沥青的60℃动力粘度时,必须严格按照试验方法的要求进行测定,以保证试验结果的准确性。     

单层多跨刚架在移动荷载作用下的影响量计算方法

讨论了桥梁、工业厂房和大型公共建筑中较多采用的单层多跨刚架在移动荷载作用下影响量的计算方法。以工程中计算连续梁的一次力矩分配法的概念和思路为基础,建立了结构中杆端真实抗转刚度和结点转角传递的概念及其相应计算公式,提出了一种单层多跨刚架超静定结构影响量的精确计算方法。算例表明,该方法较之传统的计算方法简捷,且既便于手算,也利于编制通用程序用于电算。     

用搅拌式旋转粘度计测水泥生料浆的流变性能

为了消除在粗分散体系中应用圆筒式旋转粘度计所存在的壁效应和沉降效应，尝试将Ｂｒａｂｅｎｄｅｒ型搅拌式旋转粘度计应用于水泥生料浆系统的流变性能测试。对比试验表明：这种方法测定的数据较圆筒式旋转粘度计测定的数据重现性好，更为合理。     

The viscosity of liquid water at pressures up to 32 MPa

The paper reports new, preliminary measurements of the viscosity of liquid water along two isotherms as a function of pressure up to 32 MPa. The measurements have been performed with a vibrating-wire viscometer especially modified for the purpose. The instrument has been calibrated with respect to the viscosity of water at a pressure of 0.1 MPa and a temperature of 293.15 K, for which an accurate reference value is available. With due regard to the precision of the determination of individual quantities and the accuracy of the calibration data, it is estimated that the accuracy of the present results is one of ±0.3% under all conditions.Paper dedicated to Professor Joseph Kestin.     

新型双旋流平焰烧嘴的研制与应用

介绍了一种新型双族流平焰烧嘴的设计思路、结构参数及工业试验结果。其结构特点是每个部件都易装易卸，其煤气旋流器的位置可根据煤气压力变化进行调节，无需稳焰器就可保证煤气压力在较大范围波动时，都可形成稳定的平展火焰。     

Dynamic analysis and drilling degrees of freedom

Finite element methods for dynamic analysis employing elements with drilling degrees of freedom are presented. The formulation is based on a variational principle in which displacements and rotations are interpolated independently. The issue of zero masses corresponding to rotational degrees of freedom is addressed and techniques for defining consistent and lumped rotational mass matrices are presented.